Operation of Bruker 113V
Turn on
Bolometer
Change diamond filter to position 2 before pumping
Connect pump station to the bolometer
Pump overnight using roughing pump according to instruction
Switch to turbo to get better vacuum
Precool bolometer using liquid nitrogen (fill twice to make sure it is full in both chamber) (see manual)
Precool for 15 minutes
Close the valve that connects the pumping station to the bolometer
Shutdown the pumping station according to the instruction and move it away
Blow out the liquid nitrogen from the Helium reservoir using He gas
Transport liquid He to the reservoir
Turn the diamond filter to position 1 for measurement
Turn the 3 switches on the preamplifier on
Spectrometer
Open the nitrogen gas valve (main, scanner and vent) on the wall
Close the valve that connects spectrometer to the pump
Vent the system (by ordering vent optics from the control panel)
Fire the Hg lamp
Turn on the scanner
Put in the sample assembly
Do a few test runs on the mirror and the sample to check if the level is consistent with previous runs
Evacuate the system by ordering so from the control panel
Close the vent valve
Open the valve that connects the spectrometer to the pump slowly
Do a few test runs to check if the system is stabilized to run the real experiement
Masurement…
Shut down
Turn off the three switches of the bolometer
Open the vent valve
Close the valve that connects spectrometer to the pump
Vent the system
Take the sample assembly out and put back the original lid
Close nitrogen gas valves (main, scanner and vent) on the wall
Evacuate the system by ordering so from the control panel
Open the valve that connects the spectrometer to the pump slowly
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